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| Registros recuperados : 7 | |
| 1. |  | AZEVEDO, D. B.; RENGEL, L. A.; THOMÉ, K. M.; MALAFAIA, G. C.; OSORIO, R. M. L. Estratégia competitiva de uma multinacional estrangeira na avicultura de postura no Brasil. In:CONGRESSO DA SOCIEDADE BRASILEIRA DE ECONOMIA, ADMINISTRAÇÃO E SOCIOLOGIA RURAL, 50., 2012, Vitória. Agricultura e desenvolvimento rural com sustentabilidade: anais. Vitória: SOBER: UFES, 2012. 15 p. Trabalho 97. SOBER 2012.| Biblioteca(s): Embrapa Gado de Corte. |
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| 2. | | AZEVEDO, D. B.; COMPARIN, F. P.; GEBLER, L.; THOMÉ, K. M.; OSÓRIO, R. M. L. Competitividade de um grupo de produtores da cadeia produtiva da maçã na região de Vacaria/RS. In: CONGRESSO DA SOBER, 50., 2012, Vitória, ES. Agricultura e desenvolvimento rural com sustentabilidade: anais. [Vitória]: SOBER: UFES, 2012.| Biblioteca(s): Embrapa Uva e Vinho. |
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| 5. | | OSORIO, R. M. L.; AZEVEDO, D. B.; MALAFAIA, G. C.; TEIXEIRA, L. M. A. Percepções dos especialistas frente às mudanças climáticas: Integração Lavoura-Pecuária-Floresta como alternativa sustentável à produção de alimentos, fibras e energia no agronegócio. In: CONGRESSO DA SOCIEDADE BRASILEIRA DE ECONOMIA, ADMINISTRAÇÃO E SOCIOLOGIA RURAL, 51., Belém, PA, 2013. Novas fronteiras da agropecuária no Brasil e na Amazônia: desafios da sustentabilidade: anais. Belém, PA: SOBER, 2013. 22. p| Biblioteca(s): Embrapa Gado de Corte. |
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| 7. | | AZEVEDO, D. B. de; OSÓRIO, R. M. L.; GRUNDLING, R. D. P.; MALAFAIA, G. C.; DOMINGUES, V. C.; SILVA, L. B. Stakeholders da bovinocultura de corte sustentável no Brasil. Revista em Agronegócio e Meio Ambiente, Maringá, v. 10, n. 2, p. 415-436, 2017.| Biblioteca(s): Embrapa Gado de Corte. |
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| Registros recuperados : 7 | |
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 | Acesso ao texto completo restrito à biblioteca da Embrapa Pecuária Sudeste. Para informações adicionais entre em contato com cppse.biblioteca@embrapa.br. |
Registro Completo
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Biblioteca(s): |
Embrapa Pecuária Sudeste. |
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Data corrente: |
07/07/2021 |
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Data da última atualização: |
28/09/2021 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Circulação/Nível: |
A - 2 |
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Autoria: |
SILVA, A. B. S. do; SÁ, I. P. de; MARCANO DE HIGUERA, J.; NOGUEIRA, A. R. de A. |
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Afiliação: |
ANA BEATRIZ SANTOS DA SILVA, UFSCAR; ÍVERO PITA DE SÁ, UFSCAR; JULYMAR MARCANO DE HIGUERA, UFSCAR; ANA RITA DE ARAUJO NOGUEIRA, CPPSE. |
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Título: |
Feasibility of dispersive liquid-liquid microextraction for molybdenum determination in lamb meat by MIP OES. |
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Ano de publicação: |
2021 |
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Fonte/Imprenta: |
Food Analytical Methods, v.14, 2021. |
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Páginas: |
p.496-502. |
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ISSN: |
1936-976X |
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DOI: |
https://doi.org/10.1007/s12161-020-01898-x |
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Idioma: |
Inglês |
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Conteúdo: |
The dispersive liquid?liquid microextraction (DLLME) was evaluated as a strategy to improve the MIP OES sensitivity for molybdenum determination in lamb meat. Initially, the dispersive (methanol) and extracting (tetrachloromethane) solvents were selected based on a mixture design. The best results were achieved with methanol and carbon tetrachloride as dispersive and extracting solvent, respectively. The operational parameters, such as pH, volume of dispersive and extractant solvents, and complexing agent concentration (8-hydroxyquinoline) were optimized using a Box-Behnken design. The optimal conditions were established as pH 3.8, 90 uL of carbon tetrachloride, 480 uL of methanol, and 1.09 mmol L-1 of 8-hydroxyquinoline. Besides, the use of external gas module control (EGCM) was explored to minimize the matrix effects caused by the organic solvent introduction. The accuracy of the proposed method was estimated employing a certificate reference material (bovine liver, NIST 1577c) and the obtained recovery was 92%. The limit of detection was found to be 0.20 ug g-1, and the enrichment factor was 4.5. The DLLME-MIP OES was applied for six samples of lamb meat, and the results compared to ICP-MS presented no statistical difference. Therefore, the proposed method showed satisfactory accuracy and suitable sensitivity. |
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Palavras-Chave: |
DLLME; MIP OES; Sample preparation; Trace analysis. |
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Thesaurus NAL: |
Microextraction. |
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Categoria do assunto: |
W Química e Física |
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Marc: |
LEADER 02099naa a2200253 a 4500
001 2132839
005 2021-09-28
008 2021 bl uuuu u00u1 u #d
022 $a1936-976X
024 7 $ahttps://doi.org/10.1007/s12161-020-01898-x$2DOI
100 1 $aSILVA, A. B. S. do
245 $aFeasibility of dispersive liquid-liquid microextraction for molybdenum determination in lamb meat by MIP OES.$h[electronic resource]
260 $c2021
300 $ap.496-502.
520 $aThe dispersive liquid?liquid microextraction (DLLME) was evaluated as a strategy to improve the MIP OES sensitivity for molybdenum determination in lamb meat. Initially, the dispersive (methanol) and extracting (tetrachloromethane) solvents were selected based on a mixture design. The best results were achieved with methanol and carbon tetrachloride as dispersive and extracting solvent, respectively. The operational parameters, such as pH, volume of dispersive and extractant solvents, and complexing agent concentration (8-hydroxyquinoline) were optimized using a Box-Behnken design. The optimal conditions were established as pH 3.8, 90 uL of carbon tetrachloride, 480 uL of methanol, and 1.09 mmol L-1 of 8-hydroxyquinoline. Besides, the use of external gas module control (EGCM) was explored to minimize the matrix effects caused by the organic solvent introduction. The accuracy of the proposed method was estimated employing a certificate reference material (bovine liver, NIST 1577c) and the obtained recovery was 92%. The limit of detection was found to be 0.20 ug g-1, and the enrichment factor was 4.5. The DLLME-MIP OES was applied for six samples of lamb meat, and the results compared to ICP-MS presented no statistical difference. Therefore, the proposed method showed satisfactory accuracy and suitable sensitivity.
650 $aMicroextraction
653 $aDLLME
653 $aMIP OES
653 $aSample preparation
653 $aTrace analysis
700 1 $aSÁ, I. P. de
700 1 $aMARCANO DE HIGUERA, J.
700 1 $aNOGUEIRA, A. R. de A.
773 $tFood Analytical Methods$gv.14, 2021.
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